Bruker Fourier 300 Manuals

1 pdf manual(s) Bruker Fourier 300 for free download (Document Types: Manual )

Bruker Fourier 300 Manual  [PDF] (16 pages)

  • Identifier: id-1548450
  • Brand: Bruker
  • Device: Fourier 300 Laboratory Equipment
  • Type: PDF
  • Key Aspects: Unpacking and Inspection Guidelines, System Architecture and Design Overview, Device Specifications Overview
  • UPD Date: 26.03.2026
  • Source File: 1452825.pdf
  • Pages: 16
  • Description: Device technical manual for the Bruker Fourier 300.
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  • Experiment Set-up • Click on the ‘Start’ tab in the TopSpin Menu bar • • Select by clicking on it. • • Give your experiment a NAME and an experiment number (EXPNO) • Make sure your data directory (DIR) is set to C:\data\student\nmr • Press the “Select” button next to Experiment, and choose which NMR experiment you will carry out. g
  • • • Once you have clicked on the experiment you wish to run, be sure to click the “Set selected item in editor” button. ! Note: If you change the parameter folder to nmr\par\user, you will be presented with a much more manageable set of experiments! !
  • • Choose the correct solvent from the drop down menu next to “Set solvent”. • Enter a Title for your experiment. • Click on • Click on the ‘Acquire’ tab in the TopSpin menu bar. • • Type lock in the command line at the bottom of the screen, or click on the “Lock” button. Select your deuterated solvent from the list that appears. • • Click on the “OK” button, and wait for the lock routine to finish. At the bottom left corner
  • Acquisition • Select by clicking on it. • Click on Close if the following window appears: • Wait for the receiver gain auto-adjust (rga) procedure to finish before continuing. The message “rga: finished” will appear in the lower left corner of the screen once the receiver gain has been automatically set. • Select by clicking on it. • NOTE: The 1H (16 scans) experiment will take ~2 minutes.
  • Processing • Click on the ‘Process’ tab in the TopSpin Menu bar. • • Click on • NOTE: This executes a processing program including commands such as an exponential window function ‘em’, Fourier transformation ‘ft’, an automatic phase correction ‘apk’ and a baseline correction ‘abs’. • • Expand the spectrum to include all peaks. This can be done by left clicking inside the spectrum window, and dragging from one side to the oth
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Bruker Fourier 300 Guide Loading a sample • Check your solvent height. For best shimming homogeneity, the sample height should be 5 cm. • Wipe the exterior of the tube clean using a Kimwipe. • If present, remove the cap from the top of the magnet bore. • • Type “ej” in the command line at the bottom of the screen to turn the lift on. • • Use the depth gauge to adjust the spinner height on the tube. • Carefully place your sample into the bore. Make sure air flow is on before releasing sample! • Type “ij” to turn off the lift. � �

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